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GC

35 GC GC

GC
( 5988-3466)

(GC Inlet Resource Guide)

24

GC

GC/MS
( 5988-3960)

(Maintaining Your GC/MS S

ystem)

48 GC/MS

GC/MS

GC

GC/MS

www.agilent.com/chem

www.agilent.com/chem

GC GC GC/MS LC (Maintaining Your ? GC/MS GC/MS System) ( 5988-3960) (GC Inlet Resource Guide) ? GC ( 5988-3466)

? HPLC

System) (

(Maintaining Your HPLC 5988-4269)

? 2002 4 15 5988-5847CHCN

2002

PerfectFit

Agilent GC

GC 35 GC

GC

Agilent GC
3 4 5 5 13 14 15 16 19 48 20 50 26 28 31 34 36 (FPD) 52 (FID) 55 56 (ECD) 37 38 38 38 39 43 44 (TCD) 45 (NPD)

PU

L

O L-

UT

POST ER ENCL

OS
ED

ting C leshoo G b Trou Guide

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GC GC

( (

) )

2

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GAS MANAGEMENT

GC

GC

GC GC

Kenji Yamaguchi

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3

GC

*

(0-1 ppm)

1-1000 ppm

1000 ppm-1%

1%-100%

ECD Research N/A

* = (≤99.998%) (UHP/Zero Grade) (99.999%) (Ultra-Pure Grade) (99.9995%) (Research Grade) (99.9999%)

4

www.agilent.com/chem

q

q q

(99.995%)

(99.9995+%)

q q q

GC
q q

q

GC
q q

S

q q q

GC

GC

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5

:
1= 2= 3= 4= 5= 6=

FID

ECD

ELCD

= =

MS

GC

GC

GC 56-58

6

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1/4

1/2

150 psi GC

1/8 (cc) 13X 4? – 200 MT (1 0.551 ) ( 100 GMT S S – – – 750 BMT ( 2 ) BMT-2 BMSR-1 5060-9084 250 16.3 ) 6 GMT-2-HP GMSR (Lexan) 36 (g) ( 18 (ppb) ) MT200-2 MSR-1

1/4

MT200-4 MSR-1

GMT-4-HP GMSR

BMT-4 BMSR-1

S

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2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

7

( 1520 ppb 100 30 mg

2000 psi)

GC

1/8 (mL) – 30 – 750 BOT-2 IOT-2-HP

1/4

IOT-4-HP

BOT-4

1/8 (mL) – 200 (1 – 750 ( S S – 100 (1 3 ) HT3-2 ACR – GC 5060-9096 2 ) BHT-2 BACR 2 ) HT200-2 ACR

1/4

HT200-4 ACR

BHT-4 BACR

HT3-4 ACR

8

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S

q

q

q

q

1/8 (mL) / OT3 / / / (1 – – ( GC/MS) – – 750 750 750 RMSH-2 RMSHY-2 RMSN-2 UMC-5-2 2/ 2 ) HCRMS CO 200 HMT200-2 100 OT3-2

1/4

OT3-4

Agilent OT3

HMT200-4 HCRMS CO2

RMSH-4 RMSHY-4 RMSN-4 UMC-5-2

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2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

9

q

8

q q q

18
q

q

q

— 1/8 1/4 — — 1/8 1/4 5183-4598 5183-4599 5183-4600 5183-1907 5182-9776 5182-9780

10

www.agilent.com/chem

QC+
QC+

4

RQC-P

QC+ —
( 41/8 RQC-P )

GC-1 GC-2

GC 56-58

GC-2-I GC-3 GC-4

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2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

11

1/8

GC/MS ECD NPD GC 5182-9704

2

5182-0816

5182-9705 4 ) ( 2 5183-4770

500 (1/8 Swagelok (3/ ) ) RDT-1020 RDT-1023 6

2002-2003

12

(Chromatography & Spectroscopy Supplies Reference Guide)

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GC

GC

GC GC

Spectra-Link

: 2000 sccm (4.2 scfh); (

: 70?F; )

: 30 psig GC ( 50 300 ) (psig) 2 0.5

1/8* 1/4*
*



1/8 1/8

50 12

5180-4196 5021-7107

500 psi

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13

(Spectra-Link)
q q q

1x10-5 cc/sec

1/8 1/4

36 (Spectra-Link) 36

SL-8 SL-4

5183-1941 ( 14 in., 35 cm)

GC 12

AC ( 115 V 220 V 115 V 220 V) 5182-9646 5182-9648

14

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GC

NIST-



1000 2000

5183-4779 5183-4780 (AC)

(

)

5183-4781
2000

ADM 1000
q q

ADM 2000
ADM 1000 —
q

± 3% 0 45?C -70 135?C

ADM 2000

q q q q



NIST

q q

RS-232 9V (120 220 VAC)

ADM 1000

CE 0.5 1000 mL/min

q

ADM 2000

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15

(mL/min) (%)

RS-232

ADM
ADM1000 ADM2000 ADM2000E


0.5 0.5 0.5 1000 1000 1000

*
±3 ±3 ±3 9V 120 VAC 220 VAC 220-1170 220-1171-U 220-1171-E


Veri-Flow 500 (110 V) Veri-Flow 500 (220 V) 5.0 5.0 500 500 He, H2, Ar/CH4 N2, He, H2, Ar/CH4 N2,

*
±3 ±3 110 VAC 220 VAC HVF-500 HVF-500-2

(Opti?ow)
Opti?ow 420 Opti?ow 570 Opti?ow 650
* **


50 700 5,000

**
+/- 3 +/- 3 +/- 2 9V 9V 9V HFM-420 HFM-570 HFM-650

0.1 0.5 5.0

Veri-Flow 500 Opti?ow 420

GC

56-58

2002-2003

16

(Chromatography & Spectroscopy Supplies Reference Guide)

www.agilent.com/chem

GC PerfectFit

Bryan Bente,

2002-2003 www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide)

17

GC
q

q

500













1 mL 3.6 mm* *

50 ?L

100 ?L

18

www.agilent.com/chem

q q q q q q q q q

q q q

24

q q q q q

q q q q q

MS

ECD

2 mL 500/ 2 mL 500/ 2 mL 500/ 100 ?L 100/ 1000/ 100/ 100/ 30 ?L 100/ 5182-3454 5182-0547 5181-1270 9301-0978 9301-0977 5184-3551 5182-0732 5181-3400

Viton
q q q q

32

300 ?L 100 ?L 15 ?L

www.agilent.com/chem

19

1. 2.

q q q

3.

(

PTV)

23 23/26 26/32 26/32

23/26 26 530 ?m 320 ?m 250 ?m

GC 56-58

20

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5 ?L,

? ?

1?L 0.5 ?L

? ?

? ? ?

1 ?L

10 ?L,

? ? ? ?

? ?

2 ?L

? ? ?

10 ?L,

? ? ?

? ? 5 ?L

? ? ?

250 ?m

320 ?m

1. 2.

3. 4. 5.

www.agilent.com/chem/supplies, ) Reference Library ( “How-to Video ”
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21

q

q

q

q

10

q

5-8 5 26 0.53mm

10-25%

q

q

q

0.32mm

0.25mm

22

www.agilent.com/chem

( 10 ?L 5 ?L ( 10 ?L 5 ?L Merlin )

0.53 mm

) 23-26s/42 23-26s/42 6/ 6/ 5181-3360 5181-8810

23/42 23/42

6/ 6/

9301-0725 5182-0875

4 mL 4 mL 4 mL 4 mL

144/ 12/ 144/ 25/

9301-0723 07673-40180 9301-1031 5182-0551 07673-20570

(4 7673 10 mL

)

18596-40015

(6/ ), 23/26 4 mL (144/ ), 2 mL (1,000/ ), (25/ ), (5/ ) GC

07673-60840

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Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

23

+50?C 1/81/41/4( )

1/81/420-40 mL/min 30-60 mL/min N2 He

H2

24

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6890/6850/5890

GC

*

1

1 2 11 mm** 3 4 5 Viton O 12/ 25/ 5/ 6 7 Vespel/ 1/4 1/4 10/ 10/ 50/

18740-60835 5183-4757 19243-80570 5080-8898 5080-8732 5181-3382 5080-8774 5180-4105

2 3 4

Liner

8

0.53 mm 1/8 1/4

19244-80540 19243-80530 19243-80540
6 5

9 10 11
** *? **

?

19243-00067 19234-60720

7 8

1/4 in. Vespel/ 1/4 in. Vespel/ graphite ferrule
1/4 in. nut 1/4 in. nut

0.53 mm
6890 6890/6850 Agilent’s GC GC

2/

5181-8830

Inside of Oven 9 10

1/8 in. 1/4 in. 1/8 in. oror 1/4 in stainless steel liner

(GC Inlet Resource Guide)
11

5890

EPC

19243-60570

1/8 1/4 ( )

19243-80510 19243-80520 GC 19243-60505 1/4 in. 10/ 5180-4105

56-58

www.agilent.com/chem

25

GC

50?C

q q q

0.5-3 ?L 0.10-10 mL

50:1

500:1

2-3 mL/min

26

www.agilent.com/chem/supplies, ) Reference Library ( “How-to Video ”

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(

20?C)

>0.8 mL <0.2 mL

0.5-2 ?L

10?C

>1?L 1-2?L <1?L 20-50 mL/min 20-80 sec 10-25?C >2 mL/min 2-3 mL/min

1-3 m, ( ?L

1-2 m )

GC

56-58

www.agilent.com/chem

27

q q q

(

41

)

6890/6850/5890

*

1 2 3 4 5 6 7 8 9 10 11 12 13 14 **
( ( 6890/5890 ) 6850 ) ( (

18740-60835 ** ** O **
( 6890/6850 )

**

G1544-80550 G1544-80530 G1544-20590 19251-20620 18740-20880 18740-20885

6890/6850 ) 5890 )

0.375

12/

5061-5869 18740-20800

(

3

)

19243-00067 19243-00070

2/ 2/

5181-8830 5183-4732 19251-00100

** **

6890/6850/5890

GC (GC Inlet Resource Guide)

Agilent’s GC

28

www.agilent.com/chem

q

(0.5 ?L

2.0 ?L)

q q q q

q

q

q

q

3?C

q q

0.1-2.0 ?L

50-80 cm/sec 30-50 cm/sec 12-15 mL/min

H2 He

1-3 m,

www.agilent.com/chem/supplies, ) Reference Library ( “How-to Video ”
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29

0.5m

2/ 250 ?m /Vespel /Vespel (5m (5m (5m ) ) ) 5/ 10/ 10/

5181-8830 5181-3323 5062-3514 160-2255-5 160-2325-5 160-2535-5 5181-3396

320 ?m 0.5 mm 250 ?m 320 ?m 530 ?m

0.18-0.53 mm

GC 56-58

30

www.agilent.com/chem

6890/5890

1a

1b

1c 1d

1c 1d 10/ 6/ 10 ?L

19320-80625 19245-40050 19091-63000 9301-0658
2 3 4

3 4 200 ?m 250 ?m 320 ?m 530 ?m 530 ?m 5 6 6890 GC 2/ ( ( ( ( ) ) ( ) ) )

19245-60760

19245-20510 19245-20515 19245-20525 19245-20580 19245-20780 5080-8853 5181-8830
5 6

1a 1b 2 5 mm BTO 5 mm GC (5890 (

320 mm 530 mm 50/ 50/

19245-80521 G1545-80520 5183-4760 5183-4758

5890 1a 1b
*

II GC) 7673A )
6890/5890

19245-80520 19245-20670
GC

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Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

31

(PTV)
PTV

PTV

PTV ( 2?C/sec 12?C/sec)
q q q q q q q q

PTV Peltier CO2).

(

N2,

0.1-1.5 ?L

PTV PTV 10-25?C

1.5 ?L

30-50 cm/sec

1-5 mL/min

1-3 m,

PYV www.agilent.com/chem/supplies, ) Reference Library ( “How-to Video ”

32

www.agilent.com/chem

6890 PTV
1 3

1 2 3 4 5 6 7 8 Graphpak 0.20 mm 0.25-0.33 mm 0.53 mm 9 Graphpak 0.20 mm 0.25 mm 0.32 mm 0.53 mm 10 11 PTV PTV ( Kalrez ( ) ) 10/ 10/ 10/ 10/ PTV PTV PTV CO2 N2 5/

G2617-60507 G2618-80500 18740-60835 G2617-60506 G2617-60508 G2619-60501 5182-9763 5182-9754 5182-9761 5182-9762 5182-9756 5182-9768 5182-9769 5182-9770 5062-3525 G2617-20510 G2617-60510 5182-9748 5182-9759 5182-9757 5182-9758 Viton CO2 Kalrez Graphpak 3D 5/ 3D 5182-9775 5182-9760 3150-0602 5182-9747 5182-9749 G2617-80540 PTV PTV PTV

2

4

5, 6

7 8
9 10

11

PTV

PTV PTV PTV PTV

2 mm 2 mm 1.5 mm 1.5 mm

180 ?L 200 ?L 150 ?L 150 ?L

5183-2038 5183-2036 5183-2037 5183-2041

www.agilent.com/chem

33

PTV

(≥ 2 ?L) (≤ 0.5 ?L)

4 mm

GC GC/MS 5183-4647 ( ) 6890/5973 GC/MSD 8270 EPA

5181-3316 EPC 5183-4647 O 5183-4711 350 ?C

O
O

5181-8818 ( )

34

www.agilent.com/chem

5/ (?l) 870 990 5183-4647 19251-60540 5183-4701 5183-4691

25/

5183-4702 5183-4692

800

18740-80190

5183-4699

5183-4700

800 [ (EPC)]

18740-60840

5183-4697

5183-4698

870

5183-4711

5183-4712

5183-4713

900 800 900

5062-3587 5181-3315 5181-3316

5183-4693 5183-4705 5183-4695

5183-4694 5183-4706 5183-4696

250 2 mm ( ) 250 2 mm 140 1.5 mm [ ] 990 4 mm 4 mm 4 mm , 4 mm, , 4mm, O O O O
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5181-8818

5183-4703

5183-4704

18740-80220 18740-80200

5183-4707 5183-4709

5183-4708 5183-4710

210-3003

210-3003-5

, ,

G1544-80730 G1544-80700 210-4004-5 210-4022-5 5180-4182 5180-4173 5180-4168
35

(12/ ) (10/ ) (10/ )

q

1/4
q q q q q q q q q q q q q q q q

q

q q q

GC (Agilent’s GC Inlet Resource Guide).
( 5988-3466)

36

www.agilent.com/chem

GC GC GC GC

GC

Eberhardt Kuhn,

www.agilent.com/chem

37

GC

DB-1ms, 0.25mm i.d., 30m, 0.25?m
q q

122-0132 19091S-433 122-1232 122-3832 19091N-133

HP-5ms, 0.25mm i.d., 30m, 0.25?m DB-XLB, 0.25mm i.d., 30m, 0.25?m

q

DB-35ms, 0.25mm i.d., 30m, 0.25?m HP-INNOWax, 0.25mm i.d., 30m, 0.25?m

q

q

GC

q

q

q q

q

GC 56-58

q

38

www.agilent.com/chem

(4/ ) 20 (0.5mm ≤ 0.32mm ) 10/ (1.0mm 0.45-0.53mm ) 10/ 115V 220V (
q

5181-8836 430-1020 5080-8853 5080-8773 ) 5182-9646 5182-9648

q

q

GC
q

(5/ ) (5/ ) 6 (5 )

705-0905 5181-3396 500-1200

(

0.45-0.53mm)

q

q

2-3

www.agilent.com/chem

Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

39

GC

q

– – –
q

– – 5-10
q

– –

GC

q q

8-16 10-15

q q

2000 (750 cc, 1/8” (750 cc, 1/8” ( (750cc, 1/8” ) ) (11 mm, 50/ ) ) )

5183-4780 BOT-2 BMT-2 RMSH-2 5183-4759

40

www.agilent.com/chem

q q

1-10

5-10

( )

1%
q q

DuraGuard

q q q

q q

0.5

1 5

GC

INJECTOR

DETECTOR

Guard Column

Column

Union

www.agilent.com/chem

“Consumer Products.”

www.agilent.com/chem

Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

41

(SPE) (5/ ) (5/ )
q q

5988-2685EN/CHCN 5183-4712 5183-4695 5181-3396 (5 ) 500-1200 160-2535-10 160-2255-10 430-3000

(-OH) (-SH)

(-NH)

(5/ )

q

10m, 0.53mm
q q

10m, 0.25mm – – – 0.5 1

q

q q q

GC GC 2-4
q

GC

GC
q

1-2

q

42

www.agilent.com/chem

GC GC

FID TCD NPD ECD

FPD

GC

Bernhard Rothweiler

www.agilent.com/chem

Only a small sampling of FID supplies are shown here. For a complete selection of FID supplies, see the Agilent 2002-2003 Chromatography & Spectroscopy Supplies Reference Guide.

43

(TCD)
TCD

1. 10-15 TCD 2.

TCD

6890/6850/5890 TCD TCD TCD 1.0 mm 0.5 mm (

TCD 6890/6850) 10/ G1532-60675 18740-20950 18740-20960 10/ 10/ 2/ 2/ 5080-8773 5080-8853 5181-8830 5183-4732 G1532-20710

6890 6850 TCD TCD 0.5 mL, 5890 TCD TCD TCD TCD 1/8 1/4 ( 6890/6850) C16,

3 0.3% C14 C15

18711-60060

19232-80550 19302-80020 19232-60676

44

www.agilent.com/chem

5. 1. 2. 3. 4. 1 20-100 ?L TCD 10 20-30?C 6. 30

(NPD)
q

NPD 100?C 150?C 30 30

NPD NPD
q q

6
q q q

(320 – 335?C)

NPD

www.agilent.com/chem

45

NPD ( NPD FID ) 53

NPD NPD (99.999%

)

2-3 C

NPD

FID

NPD
(mm) (0.011 ./0.29 mm ) 6890 ) 48 G1531-80560

(

6890/5890 0.53 mm (0.018 in. (0.011 in. ) ) 61.5 63.5 19244-80560 18710-20119

46

www.agilent.com/chem

(NPD)

6890 NPD 1 2 , M3 x 0.5 x 8 mm (Pozidriv) NPD NPD 3 4 5 6 7 8 9 10 11 12 13 14 15 ( 54 ) NPD NPD 16 NPD 4, 5, 7 17 18 5890 NPD NPD (NPD ) 10 19234-60540 5080-8872 19231-60790
* **

0515-0655 G1534-60570 5183-2007 G1534-80510
1 2

* **

3

C

0905-2580 G1534-40020 G1534-20530 G1534-40030
6 4 5 9 10 12 11

C M4 x 10 mm JM4 x 10 mm NPD

0905-1284 0515-2495 1400-0015 0515-2495 G1534-60610 G1531-40020
13 14

8

7

G1534-80500 G1534-80540 G1534-20590

15 16

17

8

5182-9722

18

NPD 19234-60720

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NPD Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

47

(ECD)
(ECD) 10 ) — ECD (?-ECD) ( ?-ECD

GC

(99.9995%)
63Ni

?

x-

ECD
?

48

www.agilent.com/chem

(ECD)

6890 ECD ECD * G1533-80565 19234-60720 5890 ECD 1 Vespel Vespel/ 1/4 2 3 4 5 ECD ECD ( ) ECD ECD) 3 0.5 mL 18713-60040 18713-60050
19233-20625 19233-20755
1 2

1/4 85%/15%

10/ 10/ 10/

5080-8774 0100-1331
ECD 1/4

3

1/4 ECD ECD 1/4 1/8

5180-4105 19301-80530
7

G2397-80520
6

19233-80565
5, 4

6890/5890 6 ECD ECD 7 ECD (

19233-20625 G2397-20540 19233-20755
ECD

ECD (0.033 ppm) ECD
*

GC

56-58

www.agilent.com/chem

49

(FPD)
q q

PMT PMT PMT
q

65500 GC 5A PMT FPD ( 53 FID ) 53 FPD FPD
q q

q

(PMT) PMT
q q

FPD
q

q q q

GC

50

www.agilent.com/chem

6890/5890 FPD

1 2 4 5 6 7 8 9 10 11 12 14 15 16 17 18 19 20 21 O Viton, 1.239 1/8 12/ O 12/ O 12/ M3 x 12 ( 4 ) ( 6890) O Kalrez 1/4 10/

19256-60700
1

5180-4105
3

2

19256-80560 0905-1102 19256-20590 0854-0141 G1535-60600 19256-80040 19256-80030 19256-20580 19256-20550 0515-0911 19256-00090 5061-5886 19256-80060 5061-5891 19256-20510 19256-00200 5061-5890 19256-80590 19256-80570 ( FPD O ( 5890) 5890) 12/ 19256-60500 5061-5867 19256-60590 19256-80000 19256-80010 Kalrez O Kalrez O O 0.926 FPD 3 20 ng/mL (20 ppm) 19305-60580 12/ 5061-5889 2-002 2-011 0905-1101 0905-1103
8 7 6 5

4 9 10 11

12 13 14

15

16 17 18 19 20 21

393 nm 525 nm

www.agilent.com/chem

51

(FID)

FID 100?C

FID

q

FID

FID
q

q

q

FID

FID

52

www.agilent.com/chem

(FID)

(

FID

9301-0985)

1.

6890/6850 G1531-20700 G1531-20690 FID * G1531-60690 G1531-20700

2. 5 3. 4. 5

FID

G1531-60680 G1531-20740

5890 * 19231-60690 19231-20970 19231-20960

5. GC 6. 6890/6850/5890 PTFE ( )

19231-21080 19231-20950

19231-21050 19231-20940 10/ 5181-3311 19231-20910 19231-21060 19231-60680

FID FID (5880, 5890, 6890) FID FID O FID 0.03% C14, C15 C16 1/4

2/

8710-1346 19301-00150 8710-1561 19301-60660

12/

5080-4978

18710-60170 0.03 530 mm 0.018 FID
*

5/ 5/

5180-4150 5180-4152 9301-0985

FID www.agilent.com/chem

Agilent 2002-2003 (Chromatography & Spectroscopy Supplies Reference Guide)

53

FID
(mm) FID (0.011 ( ( 6890) ) ) 48 48 G1531-80560 G1531-80620

./0.29 mm 0.018

FID (6890/6850/5890) 0.53 mm (0.018 (0.030 0.53 mm (0.018 (0.011 ) ) ) ) 61.5 63.5 63.5 61.5 19244-80560 18710-20119 18789-80070 19244-80620
FID

FID www.agilent.com/chem/supplies, ) Reference Library ( “How-to Video ”

54

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GC

35

GC

GC

Hwee-Sian Tan

www.agilent.com/chem

55

GC

GC
H5926A 6890 GC GC 4

GC

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